An efficient and convenient approach to sucrose-containing dilactams has been developed. The method, based on reaction of regioisomeric 6,6'-di--[(aminomethyl)-phenyl]-1',2,3,3',4,4'-hexa--methylsucrose with isophtaloyl or 2,6-pyridinedicarbonyl dichlorides, provided the 1:1-macrocycles in good yields.,.
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