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PMID: 4737320 Published · ppublish English Journal Article

Isocoproporphyrin: nuclear-magnetic-resonance-and mass-spectral methods for the determination of porphyrin structure.

The Biochemical journal ·Vol. 131 ·No. 2 ·1973-02-00 ·Pages 429-32

Stoll MS, Elder GH, Games DE, O'Hanlon P, Millington DS, Jackson AH

Abstract

The use of ;shift reagents' in the determination of n.m.r. spectra, and of reductive alkylation in combination with g.l.c.-mass spectrometry, facilitates assignment of the order of substituents in porphyrins, and the application of these new techniques to isocoproporphyrin is described.

MeSH Terms
Alkylation Animals Chromatography, Gas Coproporphyrins Deuterium Europium Feces Humans Ketones Magnetic Resonance Spectroscopy Mass Spectrometry Porphyrins Rats
Chemicals
Coproporphyrins Ketones Porphyrins isocoproporphyrin Europium Deuterium
Authors & Affiliations
6 authors, click to expand affiliations / ORCID
Stoll M S
Elder G H
Games D E
O'Hanlon P
Millington D S
Jackson A H
References (3)
3 references, click to expand
  1. Identification of a group of tetracarboxylate porphyrins, containing one acetate and three propionate -substituents, in faeces from patients with symptomatic cutaneous hepatic porphyria and from rats with porphyria due to hexachlorobenzene.
    Biochem J. 1972 Feb;126(4):877-91 PMID: 4116290
  2. Pyrroles and related compounds. XX. Syntheses of coproporphyrins.
    J Chem Soc Perkin 1. 1972;12:1475-83 PMID: 5065338
  3. Isolation, structure and synthesis of a tricarboxylic porphyrin from the harderian glands of the rat.
    FEBS Lett. 1970 Jan 15;6(1):9-12 PMID: 11947321
Article Info
Journal
The Biochemical journal
Abbr.
Biochem J
ISSN
0264-6021
Published
1973-02-00
Pages
429-32
Language
English
Region
England
NLM ID
2984726R
PMCID
PMC1177486
Subset
IM
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